Chemical separations : principles, techniques, and experiments

Clifton E. Meloan

Performing effective chemical separations-a step-by-step guide to the most commonly used techniques. How do experienced analysts go about making a chemical separation work? Through precise, detailed coverage of the principles, equipment, and techniques involved, this combination laboratory manual and reference source gives readers a working knowledge of an impressive array of separation methods. In forty-two chapters, it explores all major categories of separation, including those involving phase changes, extraction, chromatography, ion-exchange resins, electric fields, flotation, membranes, and miscellaneous techniques. With an emphasis on everyday practice rather than theory, Chemical Separations explains the principles and parameters of these methods with a minimum of mathematics, while providing 59 specific experiments to demonstrate proper procedures. Drawn from well-known commercial and academic laboratories and approved by national standard-setting organizations, these experiments feature step-by-step protocols for each separation scheme, precise instructions on setting up the apparatus, and helpful checklists for essential chemicals and supplies. With Chemical Separations as their guide, laboratory analysts and newcomers to chemical analysis will learn how to obtain quality analysis using commercial products, natural samples, and proven real-world laboratory techniques.

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[目次]

  • SEPARATIONS INVOLVING PHASE CHANGES. Volatilization. Zone Melting. Distillation: General Information. Azeotropic and Extractive Distillations. Steam and Immiscible Solvents Distillation. Vacuum Distillation. Molecular Distillation and Sublimation. Lyophilization (Freeze Drying). SEPARATIONS INVOLVING EXTRACTION. Extraction: General Concepts. Continuous Extraction. Countercurrent (Extraction) Chromatography: The Ito Coil-Planet Centrifugal Extractor. Solid Phase Extraction. Supercritical Fluid Extraction. SEPARATIONS INVOLVING CHROMATOGRAPHY. Chromatography: General Theory. Displacement and Multiple Column Partition Chromatography. Affinity Chromatography. Size Exclusion Chromatography (Gel Filtration
  • Gel Permeation). Flash Chromatography. High Performance Liquid Chromatography (HPLC). Gas-Liquid Chromatography. Paper Chromatography. Thin Layer Chromatography. SEPARATIONS INVOLVING ION EXCHANGE RESINS. Ion Exchange. Ion Chromatography. Ion Retardation, Ion Exclusion, and Ligand Exchange. SEPARATIONS INVOLVING ELECTRIC FIELDS. Electrodeposition. Electrophoresis--General. Immunoelectrophoresis. Polyacrylamide Gel Disc Electrophoresis. Ion Focusing, SDS, and Two-Dimensional Electrophoresis. Capillary Zone Electrophoresis. Field Flow Fractionation. SEPARATIONS INVOLVING FLOTATION. Purge and Trap and Dynamic Headspace Analysis Foam Fractionation, Gas-, and Liquid-Assisted Flotation. SEPARATIONS INVOLVING MEMBRANES. Osmosis and Reverse Osmosis. Dialysis and Electrodialysis Filtering and Sieving. SEPARATIONS INVOLVING MISCELLANEOUS TECHNIQUES. Density Gradients. Centrifugation. Masking and Sequestering Agents. Solubility. Gas Analysis by Portable Orsat. Appendices. Index.

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この本の情報

書名 Chemical separations : principles, techniques, and experiments
著作者等 Meloan Clifton E.
シリーズ名 Techniques in analytical chemistry
出版元 Wiley
刊行年月 c1999
ページ数 xv, 752 p.
大きさ 29 cm
ISBN 0471351970
NCID BA46367415
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言語 英語
出版国 アメリカ合衆国
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